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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 21, Number 6
BKCSDE 21(6)
June 20, 2000 

 
Title
A Facile Synthetic Protocol for the Preparation of 4-Halobutyl Benzoates via Carbon-Oxygen Bond Cleavage of THF
Author
Jongmin Kang, Seung-Hoi Kim
Keywords
Abstract
A facile synthetic route for the preparation of 4-halobutyl benzoates has been developed. 4-Chloro-, bromo-and iodobutyl benzoates can be easily prepared from the reaction of benzoyl chloride and metal halides in THF under extremely mild conditions. 4-Halo groups were easily controlled by selecting suitable metal halides.
Page
611 - 612
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