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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 23, Number 3
BKCSDE 23(3)
March 20, 2002 

 
Title
α-Cyclodextrin Modified Screen Printed Graphite Electrodes for Detection of Phenols
Author
Hwa-jeong Kim, Seung-Cheol Chang, Yoon-Bo Shim
Keywords
a-Cyclodextrin, Phenols, Screen printed electrode, Voltammetry.
Abstract
A screen printed graphite electrode has been developed for a simple and sensitive determination of phenolic compounds in an aqueous solution. The electrode developed uses a simple and effective screen printing technique with α-Cyclodextrin(α-CD) modified graphite ink. Phenols were captured on the surface of the α-CD modified electrode through complex formation. The phenol/ α-CD complex was deposited and quantified electrochemically using cyclic voltammetry (CV), differential pulse voltammetry (DPV) and square wave voltammetry (SWV). The optimization of the experimental parameters was performed in regard to electrode composition, pH, temperature, sample preconcentration time. Interferences from other organic compounds were investigated. The detection limit for phenols was 500 ±7 nM for DPV, with the linear range of 0.5 μM -25.0 μM and 30 ±2 nM for SWV, with the linear range of 30 nM - 50μM, respectively.
Page
427 - 431
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