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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 29, Number 5
BKCSDE 29(5)
May 20, 2008 

 
Title
Simultaneous Determination of Amitraz, Bromopropylate, Coumaphos, Cymiazole and 2,4-Dimethylaniline in Korean Honey Samples by High-Performance Liquid Chromatography
Author
Jae Jeong Ryoo*, Se Hoon Kim, Young Han Jeong, Hwan-Suk Do, Jeong Eun Ryu, Hae Young Kwon, Ji Yoon Jeong, Hye Jin Park, Soon Ho Lee, Moo Ki Hong, Jongki Hong
Keywords
Simultaneous analysis, Honey, Acaricide, HPLC-UV
Abstract
Simultaneous determination of amitraz, bromopropylate, coumaphos, cymiazole and 2,4-dimethylaniline in 200 honey samples purchased in Korea was performed by reversed-phase high-performance liquid chromatography with multiple UV detection. 2% Acetone in hexane was used for a liquid-liquid extraction and 20-40% water in acetonitrile solutions were used as mobile phases. The LOD for the analytes varied between 0.4 and 1.5 μg/L and the recoveries were yielded between 64 and 94%. Relative standard deviation of the repeatability of the method is less than 15%. Amitraz was not present in amount above 10 μg/L and one for coumaphos and cymiazole and two for bromopropylate, and three for 2,4-dimethylanilne were detected in amount above 10 μg/ L. Levels of the acaricide residues found were less than 50 μg/L.
Page
1043 - 1047
Full Text
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