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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 30, Number 1
BKCSDE 30(1)
January 20, 2009 

 
Title
A Sensitive Procedure for the Rapid Determination of Mandelic Acid by Flow Injection Analysis and Chemiluminescence Detection
Author
Seikh Mafiz Alam, Chi Wan Jeon, Mohammad Mainul Karim, Sang Hak Lee*,Saikh Mohammad Wabaidur, Yeoun Suk Suh, Hye Young Chung
Keywords
Chemiluminescence, Flow-injection analysis (FIA), Mandelic acid
Abstract
A rapid and sensitive chemiluminescence (CL) method using flow-injection (FI) has been developed for the determination of mandelic acid which is based on the enhancement of mandelic acid to the CL intensity of Ru(bipy) 32+-Ce(IV) system. The enhancement effect was dependent on the concentration of mandelic acid, based on which, CL system was established for the determination of mandelic acid. The concentrations of Ru(bipy)32+, Ce(IV), and H2SO4 were optimized. Under the optimum experimental conditions, the linear range and detection limit are 1.46-342.0 μg/mL and 0.072 μg/mL, respectively. The correlation coefficient (R) was 0.99732. The utility of this method was demonstrated by determining mandelic acid in capsules and human urine sample.
Page
102 - 106
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