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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 31, Number 2
BKCSDE 31(2)
February 20, 2010 

 
Title
Synthesis, Characterization and Catalytic Activity of Ce1MgxZr1-xO2 (CMZO) Solid
Heterogeneous Catalyst for the Synthesis of 5-Arylidine Barbituric acid Derivatives
Author
Sandip B Rathod, Anil B Gambhire, Balasaheb R Arbad, Machhindra K Lande*
Keywords
Co-precipitation method, CMZO, Knoevenagel condensation, Solvent-free, Microwave
Abstract
A series of Ce1MgxZr1-xO2 (CMZO) mixed metal oxide with different molar ratio were prepared by simple co-precipitation method. The prepared materials were tested for their catalytic activity performance using Knoevenagel condensation of various aromatic aldehydes with barbituric acid under solvent-free condition in microwave. The best catalytic activity was obtained with CMZO (1:0.6:0.4). The synthesized materials were characterized by using XRD, FT-IR, SEM-EDS techniques.
Page
339 - 343
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