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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 61, Number 4
JKCSEZ 61(4)
August 20, 2017 

 
Title
A Simple, Efficient, Catalyst-Free and Solvent-Less Microwave-Assisted Process for N-Cbz Protection of Several Amines
Author
ABSTRACT A simple, green, chemo selective method for the N benzyloxycarbonylation of amines, β amino alcohols, α amino esters, sulfonamides has been developed under microwave irradiation Good to excellent yields of the N benzyloxycarbamates com
Keywords
Amine, Benzyl chloroformate (Cbz-Cl), Protection, Microwave-assisted, Solvent-free
Abstract
A simple, green and chemo-selective method for the N-benzyloxycarbonylation of amines, β-amino alcohols, α- amino esters and sulfonamides has been developed under microwave irradiation. Good to excellent yields of the N-benzyloxycarbamates compounds were obtained in short times without any side products.
Page
151 - 156
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