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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 27, Number 11
BKCSDE 27(11)
November 20, 2006 

 

1727  

Regiospecific Addition of Alkyl and Allyl Groups to α,β-Unsaturated Carbonyl Compounds with Trialkylboranes through the Palladium Catalyst
Chung Min Park, Sam Yong Han, Nan Young Seo, Chang-ho Byun, Young Soo Gyoung*
Keywords: α,β-Unsaturated carbonyl compounds, Trialkylboranes, Palladium, Three component coupling
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1727

Abstract | Full Text: PDF


1729  

Rational Design, Exploratory Synthesis and Lanthanide Emission Efficiency Comparison of Lanthanide(III)-cored Complexes Based on Naphthalene Acid Ligands for Efficient Energy Transfer Pathways
Nam Seob Baek, Yong Hee Kim, Hwan Kyu Kim*
Keywords: Naphthalene acid, Lanthanide complexes, Near-infrared emission, Energy transfer process
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1729

Abstract | Supporting Information | Full Text: PDF


1731  

Replication Protein A from Saccharomyces cerevisiae Differently Binds to Photo-damaged DNA from Normal Single-stranded DNA
Joon-Hwa Lee, Chin-Ju Park, Byong-Seok Choi*
Keywords: NMR, Replication protein A, Damaged DNA, Chemical shift mapping, cis-syn Cyclobutane pyrimidine dimer
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1731

Abstract | Full Text: PDF


1733  

Purification and Characterization of [Ala2]-Neuromedin N from the Visceral Tissue of the African Lungfish, Protopterus dolloi
Chan-Hee Kim, Hye-Jin Go, Eun Jung Kim, Jung-Kil Seo, Yong-Ki Hong, Hyung-Rak Kim, Joon-Ki Chung, Yojiro Muneoka, Nam Gyu Park*
Keywords: African lungfish, Purification, [Ala2]-Neuromedin N
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1733

Abstract | Full Text: PDF


1737  

DFT Study of Bis(Crown-Ether) Analogue of Troger’s Base Complexed with Bisammonium Ions: Hydrogen Bonds
Kwangho Kim, Jong-In Choe*
Keywords: DFT B3LYP/6-31G(d,p), Bis(crown-ether), Bisammonium ion, Complex
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1737

Abstract | Full Text: PDF


1741  

CoMFA and CoMSIA on the Neuroblocking Activity of 1-(6-Chloro-3-pyridylmethyl)-2-nitroiminoimidazolidine Analogues
Nack-Do Sung*, Seok-Chan Jang, Kyoung-Seop Choi
Keywords: Imidacloprid analogues, Neuroblocking activity, CoMFA, CoMSIA analysis
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1741

Abstract | Full Text: PDF


1747  

Synthesis and Characterization of Dinuclear Ni(II) Complexes with Tetraazadiphenol Macrocycle Bearing Cyclohexanes
Ki Ju Kim, Duk Sang Jung, Duk Soo Kim, Chi Kyu Choi, Ki Min Park, Jong Chul Byun*
Keywords: Tetraazadiphenolic macrocycle, Macrocyclic nickel(II) complex, Crystal structure, Isothiocyanato ligand
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1747

Abstract | Full Text: PDF


1752  

An NMR Study of Solvent Interactions in a Paramagnetic System
R. M. Golding*, R. O. Pascual, C. Suvanprakorn, I. G. Dance
Keywords: NMR paramagnetic chemical shifts, Tris(N,N-diethyldithiocarbamato) iron(III), Electronnuclear interactions, Solvent-solute interactions
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1752

Abstract | Full Text: PDF


1757  

Fundamental Study on Solvent Sublation Using Salphen and Its Application for Separative Determination of Trace Ni(II), Co(II) and Cu(II) in Water Samples
Young-Sang Kim*, Gyo In, Mi-Hyun Kim, Jong-Moon Choi
Keywords: Solvent sublation, Salphen, Nickel(II), Cobalt(II), Copper(II)
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1757

Abstract | Full Text: PDF


1763  

Electrocatalytic Reduction of Molecular Oxygen at Poly(1,8-diaminonaphthalene) and Poly(Co(II)-(1,8-diaminonaphthalene)) Coated Electrodes
Hyun Park, Tae-guen Kwon, Deog-Su Park, Yoon-Bo Shim*
Keywords: Conductive polymer, Metal complex polymer, Electrocatalytic reduction of O2
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1763

Abstract | Full Text: PDF


1769  

Preparation of a New Chiral Stationary Phase Based on (2S,3S)-O,O'-Bis-(10-undecenoyl)-N,N'-bis-(3,5-dinitrobenzoyl)-2,3-diamino-1,4-butandiol and Its Application for the Liquid Chromatographic Resolution of Enantiomers
Myung Ho Hyun*, Chang Jin Boo, Hee Jung Choi, Yun Kyoung Kim, Bu Sung Kang, Hyun Ju Ha, Min Ki Choi, Guanghui Tan
Keywords: Chiral stationary phase, Enantiomer separation, Liquid chromatography
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1769

Abstract | Full Text: PDF


1775  

Resolution of β-Amino Acids on a Chiral Stationary Phase Based on (+)-(18-Crown-6)-2,3,11,12-tetracarboxilic Acid without Extra Free Aminopropyl Groups on Silica Surface: the Effect of Ammonium Ion Mobile Phase Modifier on the Resolution Behaviors
Myung Ho Hyun*, Hee Jung Choi, Bu Sung Kang, Guanghui Tan, Yoon Jae Cho
Keywords: β-Amino acids, Chiral stationary phase, Enantiomer separation, Liquid chromatography
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1775

Abstract | Full Text: PDF


1780  

Determination of Mefenamic Acid in Human Urine by Means of Two Spectroscopic Methods by Using Cloud Point Extraction Methodology as a Tool for Treatment of Samples
Ahad Bavili Tabrizi
Keywords: Mefenamic acid, Cloud point extraction, Spectrofluorimetry, Spectrophotometry, Urine
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1780

Abstract | Full Text: PDF


1785  

Determination of Hydroperoxyl/superoxide Anion Radical (HO2/O2ㆍ-) Concentration in the Decomposition of Ozone Using a Kinetic Method
Bum Gun Kwon, Jai H. Lee*
Keywords: Hydroperoxyl radical, Superoxide anion radical, Ozone, Fenton-like, Hydroxyl radical
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1785

Abstract | Full Text: PDF


1791  

Enantioselective Carboxylate Receptor Using Glycoluril Molecular Scaffold
Hyungil Kim, Jongmin Kang*
Keywords: Glycoluril, Enantioselection, Amino acids
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1791

Abstract | Full Text: PDF


1795  

Convergent Synthesis of PAMAM-like Dendrimers from Azide-functionalized PAMAM Dendrons
Jae Wook Lee*, Jung Hwan Kim, Byung-Ku Kim, Ji Hyeon Kim, Won Suk Shin, Sung-Ho Jin, Myunghak Kim
Keywords: Alkyne, Azide, Click chemistry, PAMAM dendrimers, 1,2,3-Triazoles
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1795

Abstract | Full Text: PDF


1801  

Comparative and Structural Analysis of the Interaction between β-Lactoglobulin type A and B with a New Anticancer Component (2,2'-Bipyridin n-Hexyl Dithiocarbamato Pd(II) Nitrate)
A. Divsalar, A. A. Saboury*, H. Mansoori-Torshizi, B. Hemmatinejad
Keywords: β-Lactoglobulin, Pd(II) complex, Chemometry analyses, Fluorescence quenching, Binding site
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1801

Abstract | Full Text: PDF


1809  

Synthesis of the Water Dispersible L-Valine Capped ZnS:Mn Nanocrystal and the Crystal Structure of the Precursor Complex: [Zn(Val)2(H2O)]
Cheong-Soo Hwang*, Narae Lee, Young-Ah Kim, Youn Bong Park
Keywords: Crystal structure of zinc valinate complex, ZnS:Mn nanocrystal, Water dispersible nanocrystal, Amino acid capping ligand, Single molecular precursor
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1809

Abstract | Full Text: PDF


1815  

Conducting Properties of Polypyrrole Coated Imogolite
Yunha Lee, Bumjoong Kim, Whikun Yi, Atsushi Takahara, Daewon Sohn*
Keywords: Imogolite, Polypyrrole, Conducting polymer, Nano tube
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1815

Abstract | Full Text: PDF


1819  

Adsorption Kinetics for Polymeric Additives in Papermaking Aqueous Fibrous Media by UV Spectroscopic Analysis
Sung-Hoon Yoon*, Xin-Sheng Chai
Keywords: Spectroscopic analysis, Polymer adsorption, Fiber, Wet-strength resin, Softener
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1819

Abstract | Full Text: PDF


1825  

Effects of Solvent Viscosity on Conformational Dynamics of Heme-pocket in Myoglobin and Hemoglobin
Seongheun Kim, Manho Lim*
Keywords: Conformational dynamics, Heme proteins, Heme pocket, Time-resolved IR spectroscopy, Trehalose
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1825

Abstract | Full Text: PDF


1832  

Sorption of Thiocyanate Silver Complexes and Determination of Silver by Diffuse Reflectance Spectroscopy
O. N. Kononova*, N. G. Goryaeva, T. V. Vorontsova, T. A. Bulavskaya, S. V. Kachin, A. G. Kholmogorov
Keywords: Silver, Ion exchange, Thiocyanate complexes, Diffuse reflectance spectroscopy
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1832

Abstract | Full Text: PDF


1839  

Lanthanide-Oxalate Coordination Polymers Formed by Reductive Coupling of Carbon Dioxide to Oxalate: [Ln2(3,5-pdc)2(C2O4)(H2O)4]·2H2O (Ln = Eu, Sm, Ho, Dy; pdc = Pyridinedicarbox
Hyun Sue Huh, Soon W. Lee*
Keywords: Lanthanide, Oxalate formation, Hydrothermal reaction, X-ray diffraction
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1839

Abstract | Full Text: PDF


1844  

Dehydration of Methanol to Dimethyl ether, Ethylene and Propylene over Silica-Doped Sulfated Zirconia
Syed T. Hussain*, M. Mazhar, Sheraz Gul, Karl T Chuang, Alan R. Sanger
Keywords: Sulfated zirconia, Dehydration of methanol, Dimethyl ether, Ethylene, Propylene
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1844

Abstract | Full Text: PDF


1851  

XPS Investigation of A3 Coupling Reaction in Room Temperature Ionic Liquids
Ji Hye Kwon, So Won Youn, Yong-Cheol Kang*
Keywords: X-ray photoelectron Spectroscopy, Ultra-high vacuum, A3 coupling reaction, Room temperature ionic liquid
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1851

Abstract | Full Text: PDF


1854  

Electrochemical Investigation of Acetaminophen with a Carbon Nano-tube Composite Film Electrode
Chunya Li*, Guoqing Zhan*, Qingdan Yang, Jianjie Lu
Keywords: Acetaminophen, Multi-wall carbon nano-tube, Electroanalysis
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1854

Abstract | Full Text: PDF


1861  

Synthesis of Piperazinylalkylisoxazoline Analogues and Their Binding Affinities for Dopamine Receptor Subtypes
Ji Young Jung, Sun Ho Jung*, Hun Yeong Koh*, Ae Nim Pae, Woo-Kyu Park, Jae Yang Kong
Keywords: Dopamine receptors, Piperazinylalkylisoxazolines, Combinatorial synthesis, Reductive amination, 1,3-Dipolar cycloaddition
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1861

Abstract | Full Text: PDF


1865  

DFT Studies on Hydrolyses of Dimethylchlorothiophosphate
Young Hee Park, Oh-Seuk Lee, In Sun Koo, Kiyull Yang*, Ikchoon Lee
Keywords: Density functional theory, Hydrolyses, Dimethylchlorothiophosphate
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1865

Abstract | Full Text: PDF


1869  

Preparation of Cu Nanoparticles from Cu Powder Dispersed in 2-Propanol by Laser Ablation
Jaehoon Lee, Dong-Kuk Kim, Weekyung Kang*
Keywords: Cu nanoparticle, Laser ablation, 2-Propanol
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1869

Abstract | Full Text: PDF


1873  

Kinetics and Mechanism of the Addition of Benzylamines to Benzylidenedimethylmalonates in Acetonitrile
Hyuck Keun Oh*, Myoung Hwa Ku
Keywords: Nucleophilic addition reaction, Single-step process, Cross-interaction constant, Kinetic isotope effects, Four-center cyclic transition state
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1873

Abstract | Full Text: PDF


1877  

Preparation and Characterization of Nicotinium Tetrahalocuprate(II) and Tetrahalocobaltate(II) Complexes : Structure of Nicotinium Tetrachlorocobaltate(II)
Sung-Kwon Kang, Hyun-Sook Kim, Young-Inn Kim*
Keywords: Nicotine complexes, Tetrahalocuprate(II), Tetrahalocobaltate(II), Bifurcated hydrogen bond
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1877

Abstract | Full Text: PDF


1881  

Spherical Self-aggregates Formed with an Alanine-functionalized Porphyrin Derivative in Organic Solvent
Eun Jin Cho, Jeung Ku Kang, Sunwoo Kang, Jin Yong Lee*, Jong Hwa Jung*
Keywords: Self-Assembly, Porphyrin, Spherical, Alanine
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1881

Abstract | Supporting Information | Full Text: PDF


1885  

Study of an Enzyme Activity in Extracts of Ginkgo biloba Leaves
Seongsoon Park
Keywords: Ginkgo extracts, Peroxidase, Biocatalyst
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1885

Abstract | Full Text: PDF


1888  

Synthesis of Styrylquinoline Carboxamides for HIV-1 Integrase Inhibitors
Seung Uk Lee, Jang Hyun Park, Jae Yeol Lee, Cha-Gyun Shin, Bong Young Chung, Yong Sup Lee*
Keywords: HIV integrase, Inhibitor, Styrylquinoline, 3'-Processing, Strand transfer
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1888

Abstract | Full Text: PDF


1891  

Carnosine and Homocarnosine Inhibit Cytochrome c-Mediated DNA Strand Breakage
Jung Hoon Kang
Keywords: Cytochrome c, DNA, Peroxidase
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1891

Abstract | Full Text: PDF


1894  

Synthesis of Novel Poly(amido ethylenimine) (PAMEIM) Dendrimer and Its Self-assembly with Plasmid DNA
Tae-il Kim, Jung-un Baek, Cheng Zhe Bai, Jong-sang Park*
Keywords: Gene delivery carrier, Dendrimer, Self-assembly
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1894

Abstract | Full Text: PDF


1897  

Synthesis and Fluorescence Behavior of Cation Chemosensor Based on Azacrown Ether Fluoroionophore Carrying Styrylanthracene
Eun Ju Shin
Keywords: Azacrown ether, Chemosensor, Styrylanthracene, Fluoroionophore
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1897

Abstract | Full Text: PDF


1900  

Synthesis of Symmetric Diallyl Disulfides from Baylis-Hillman Acetates
Myeong Jong Cha, Young Seok Song, Kee-Jung Lee*
Keywords: Baylis-Hillman reaction, Thiols, Thiolacetylation, Diallyl disulfides
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1900

Abstract | Full Text: PDF


1903  

The Structures and Proton Transfer Barriers in Proton-bound Homodimers of Aromatic Molecular Bases: Implication of Zero-point Energies for the Proton-transfer Reaction
Sang Yun Han*, Sang Hak Lee, Han Bin Oh
Keywords: Density functional calculations, Proton-bound dimer, Pyrazine (C4H4N2), Quinone (C6H4O2), Zero-point energy
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1903

Abstract | Full Text: PDF


1907  

Aluminium Phthalocyanine: An Active and Simple Catalyst for Cyanosilylation of Ketones
Gurusamy Rajagopal, Sung Soo Kim*, Ju Myung Kwak
Keywords: Cyanohydrins, Catalysis, Ketones, Aluminium phthalocyanine, Triphenylphosphine oxide
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1907

Abstract | Full Text: PDF


1910  

An Efficient Synthesis of Thiophene/Pyrrole-Fused Crown Ethers Using Mitsunobu Reaction for Potential Application to Sensory Electroactive Polymers
Joongchul Kim, Daehyun Yoon, Sang Hee Lee, Seokbeom Ko, Youn-Sik Lee, Kyukwan Zong*
Keywords: Thiophene, Pyrrole, Conjugated polymer, Crown ether, Mitsunobu reaction
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1910

Abstract | Full Text: PDF


1913  

New Synthetic Method of Aldehydes from Tertiary Amides by Lithium Diisobutylpiperidinohydroaluminate (LDBPA)
Su Mi Woo, Min Eai Kim, Duk Keun An*
Keywords: Lithium diisobutylpiperidinohydroaluminate (LDBPA), Aldehyde, Tertiary amide, Piperidine, Diisobutylaluminium hydride (DIBAH)
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1913

Abstract | Full Text: PDF


1915  

Anion-Controlled Copper(II) Coordination Polymers Based on Angular Dipyridyl Ligand
Yong Woon Shin, Tae Ho Kim, Joobeom Seo, Shim Sung Lee, Jineun Kim*
Keywords: Dipyridyl ligand, Self-assembly, Crystal structure, Anion effect, Copper(II) coordination polymer
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1915

Abstract | Full Text: PDF


1919  

A Structure-Based 3D-QSAR(CoMSIA) Study on a Series of Aryl Diketoacids (ADK) as Inhibitors of HCV RNA-dependent RNA Polymerase
Jinyoung Kim, Jin Hee Han, Youhoon Chong*
Keywords: HCV RdRp, Aryl diketoacid (ADK), FlexX-Pharm, CoMSIA
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1919

Abstract | Full Text: PDF


1923  

Method Validation for HPLC Assay of 7-Chloro-1-cyclopropyl-fluoro-1,4-dihydro-4-oxo-1,8-naphthylidine-3-carboxylic acid
Hoonjoo Kim*, Youngsuk Kim, Dongmin Kim, Chan-Wha Kim
Keywords: Method validation, HPLC
DOI: https://doi.org/10.5012/bkcs.2006.27.11.1923

Abstract | Full Text: PDF